Characterisation data for 'Ultrasound-assisted continuous aqueous synthesis of sulfonate, imidazolate, and carboxylate MOFs with high space time yield'

Metal–organic frameworks exhibit promising properties for applications from gas separations to energy applications. Yet scale-up with non-toxic solvents remains a challenge. Combining the increased heat and mass transfer of flow reactors with the enhanced mixing and nucleation rates of sono-chemical synthesis, we developed an ultrasound-assisted two-phase flow platform for the aqueous synthesis of MOFs spanning three ligand chemistries, sulfonate Ca-NDS (water), imidazolate ZIF-8, and carboxylate UiO-66-NH2. This dataset includes the characterisation data supporting these results, highlighting the potential of ultrasound-assisted flow synthesis for MOFs.